库仑计C语言程序,ASTM C1165-2017 用控制电位库仑计法在铂工作电极上测定-CSDN博客

该测试方法用于确定材料是否符合钚含量或钚分析规格，适用于未辐照的铀钚混合氧化物中毫克级钚的测定，也适用于钚金属、钚氧化物、钚碳化物等各种钚化合物和溶液。化学校准对于获得准确结果至关重要。此标准适用于保障和核安全应用，但不涵盖所有安全问题，使用者需在使用前确定适当的安全、健康和环境实践，并考虑法规限制。

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5.1x00a0;This test method is to be used to ascertain whether or not materials meet specifications for plutonium content or plutonium assay, or both.

5.2x00a0;A chemical calibration of the coulometer is necessary for accurate results.

FIG. 1 Example of a Cell Design Used at Los Alamos National Laboratory (LANL)

5.3x00a0;Fitness for Purpose of Safeguards and Nuclear Safety Applicationx2014;Methods intended for use in safeguards and nuclear safety applications shall meet the requirements specified by Guide C1068 for use in such applications.

1.1x00a0;This test method covers the determination of milligram quantities of plutonium in unirradiated uranium-plutonium mixed oxide having a U/Pu ratio range of 0.1 to 10. This test method is also applicable to plutonium metal, plutonium oxide, uranium-plutonium mixed carbide, various plutonium compounds including fluoride and chloride salts, and plutonium solutions.

1.2x00a0;The recommended amount of plutonium for each aliquant in the coulometric analysis is 5 to 10 mg. Precision worsens for lower amounts of plutonium, and elapsed time of electrolysis becomes impractical for higher amounts of plutonium.

1.3x00a0;The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.4x00a0;This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 9.

1.5x00a0;This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.