在运行rxn4chemistry 的from chemdataextractor import Document.py
from chemdataextractor import Document
doc = Document('To a mixture of Cu(OAc)2.H2O (0.01 mmol, 1.0 mol%) and 1,2- bis(diphenylphosphaneyl)benzene (0.015 mmol, 1.5 mol%) in an oven dried Schlenk tube connected to a CO2 balloon, a solution of PMHS (cas: 613-152-3, 2.5 mmol, 2.5 equiva.) in 1,4-dioxane (2.0 mL) was added, flushed the tube with CO2 and heated the resulting blue solution to 65 ℃ while vigorously stirring for 20 minutes under balloon pressure CO2 and the solution becomes light brown. This formate solution was removed from the heating bath and added toluene (8 ml), 1-chloro-4-nitrobenzene (1.0 mmol, 1.0 equiv.), Pd(OAc)2 (3 mol%, 0.03 equiva.), xantphos (6 mol%, 0.06 equiva.) and Et3N (2.5 mmol, 2.5 equiva.) sequentially under CO2 atmosphere. CO2 was removed, the Schlenk tube was closed and heated to 100 ℃ for the time period until the disappearance of aryl chloride as shown by TLC. Then,